Parr-instrument 1356 Manuale Utente

No. 434M 1356 ISOPERIBOL BOMB CA

10 nitrogen that was present as part of the air trapped in the bomb is burned to nitric oxide which combines with water vapor to form nitric a

11 Spiking Calculations [{EE x T(temp rise)}-e1-e2-e3-[mass(oil) x Heat Combustion(oil)]/sample m grams 2. 1108 Oxygen Bomb Maintenance and Safe

12 Sample preparation

13 the 238A sealing ring ages and hardens it becomes a partial electrical conductor, permitting misfires and producing unwanted heating effects.

14 2. Parts Replacement Keyboard A bad keyboard panel will result in the calorimeter responding to only some rows or columns of keys and ignor

15 the left side panel via velcro and is located between the power supply board at the front and the cpu board and is connected electrically to th

16 4. Remove the six screws located on the display bezel and remove the bezel. 5. Push the rear of the controller near the bottom of the cas

17 12. Position the new mounting plates on the shaft assembly rod. Raise the shaft assembly rod to position the support rod mounting plate ove

188. Misfire Error Ignition Problems on the 1356 Calorimeter are generally attributed to one of three possible sources, after having checked

19 Low Oxygen Charge Low Oxygen Pressure - signifies low oxygen pressure in the line filling the bomb. The

20 Oxygen Use P1A Oxygen Cylinder volume of cylinder 43.8 liters pressure of cylinder 2490 psi V x P = 109062 liters-psi Amount of gas

21 1. Solid Fuels (D2015) Heat of Formation of ... 29KJ/mole Sulfuric Acid for a Fuel with 5% sulfur and 5% hydrogen S02(g) + 1/2 02(g) + H20(1

22 4. Nitrogen 1.251 gm x 10.8 liter = 13.51 gm .249 cal x 13.51 gm = 3.36 cal gm K K oxygen 3.4 cal/C argon 2.4

231356 Data Logger To log data one may either log the data to the internal ram disc, or send the data directly to the printer or to the computer.

24 The 1356 Calorimeter Controller can be physically separated into two halves. The upper part consists of the keyboard, LCD display, keypad and disp

25 Lengthening Post Period for 1356 Calorimeter Gain entry to the factory menu by pressing the following three keys simultaneously from the main m

26 attached to the display. Set the display to the side. Care should be taken to avoid scratching the display. 4. Remove the 5 screws holding

27 1356 Calorimeter Parts List Item Description Item Description 421A A476A3 393DD 1027DD 539DD 549DD 558DD

28 Recommended Spare Parts Per 5000 Tests Qty. Part No. Description 3 PKG (2) 3 PKG (2) 1 PKG (12) 3 PKG (12) 1 PKG (2) 1 PKG (2) 1 3 PKG (2)

29 Parts Hinge Assembly Qty Part No Description 1 A525DD Lower RH Link 1 A526DD Lower LH Link 2 527DD Li

1. Calorimeter Operation Operation……………………………………………………………………5 Corrections Fixed………………………………………………………… 6 Corr

30 Parts List 1563 Water Handling System Part No. Description 108C 110C 148C 149C 186DD 612DD A633DDEA A633DDEF 894DD 34E2 138E 178E 185E 20

31 1356 Calorimeter Front View SA1332RD06Lower L

32

33 A546DD2 Left Bracket Linkage

34 A535DD3 Right Mounting Plate

35 A545DD2 Right Bracket Link

36 1356 Cover Assembly Assembly

Diagram Flow

Electrical Diagrams Water Handling

39 MSDS-Benzoic Acid ----------------------------------------------------------------------- 1 - PRODUCT IDENTIFICATION ------------------------

4 MSDS sheet benzoic acid…………………………………………………. 41

40 FIRE EXTINGUISHING MEDIA USE ALCOHOL FOAM, DRY CHEMICAL OR CARBON DIOXIDE. (WATER MAY BE INEFFECTIVE.) SPECIAL FIRE-FIGHTING PROCEDURES FIR

41----------------------------------------------------------------------- 7 - SPILL AND DISPOSAL PROCEDURES --------------------------------------

5 1. Calorimeter Operation A. Operating the Calorimeter

6 Press the START key . The calorimeter will prompt for a Cal ID. The calorimeter will then prompt for sam

7 B. Entering Corrections and Obtaining the Final Report Final reports for each test can be obtained via the REPORT key, whenever the user is pr

8 Reports may be obtained by pressing the REPORT key. To obtain a block of reports between two specified sample numbers, press the REPORT key.

9 Press the Clear key, enter the new value on the keyboard and press the Enter key. This sequence is canceled by pressing the RESET key. Press